Dedicated NMR Instrument for Reaction Monitoring, 500 MHz, Bath

Dedicated NMR Instrument for Reaction Monitoring, 500 MHz, Bath

Dr John Lowe, NMR website

Department of Chemistry, University of Bath, Claverton Down, Bath BA2 7AY

Unusual feature: Dedicated to reaction monitoring. The core of the system is a computer-controlled recirculating batch reactor coupled to a 500 MHz NMR spectrometer with cryoprobe and equipped with flow capability. This is augmented by a range of orthogonal analytical techniques including MS, UV-vis, HPLC and IR.

¹H frequency: 500 MHz

Console type and age: Bruker AVHD, early 2017

Probe: Prodigy BBO cryoprobe, early 2017

Temperature range: -40 to 80 °C

Approximate number of hours per week for shared usage: 8, from May 2017