Bruker Avance III 300

Check the queue on the 300 MHz instrument (User ID: supervisor’s initials).

A broadband fluorine observe (BBFO) double-resonance probe has been in use since July 2022. The X-nuclei broadband frequency range covers 97Mo-31P and, additionally, includes 19F. This enables observation of 19F with 1H decoupling and vice versa.

The sensitivity specifications are: 

1H  173 : 1 (noise [200 Hz], 0.1% Ethylbenzene in CDCl3);
13C 140 : 1 (noise [40 ppm], ASTM, 40% dioxane, 60% C6D6);
15N  20 : 1 (noise [2 ppm], 90% formamide in DMSO-d6);
19F  308 : 1 (noise [1 ppm], 0.05% TFT in CDCl3);
 31P 127 : 1 (noise [5 ppm], 0.0485 M Triphenyl Phosphate (TPP) in acetone-d6).

The 300 MHz instrument is equipped with a 60-position sample changer (SampleCase Plus), shown below, together with the 300 MHz magnet and the workstation.