Fluorine and Phosphorus Triple Resonance Experiments

Dr Tomas Lebl, NMR website

University of St Andrews, KY16 9ST

Unusual feature(s): 19F triple resonance experiments, 31P triple resonance experiments and high temperature.

1H frequency: 500 MHz and 300 MHz Console type and age:

     triple-channel AVIII-HD with 2 high frequency amps, 1 year 

     triple channel AV, about 15 years old  

Probe(s), nuclei, gradients, age: 

     5mm 19F-TBO (1H,19F, BB)

     10 mm 1H,13C, 31P-TXO

Temperature range: in theory -150 - 150 oC

Approximate number of hours per week for shared usage in

     Aug-Oct: 24 h in August (Sep and Oct can be quite busy)

     Nov-Jan: 24h Jan (Nov and Dec are busy months)

     Feb-Apr: 0

     May-Jul: 24h

Staff availability for sample preparations: No. We do not have facilities to prepare samples directly in the lab. Access to a fume-hood and other equipment can possibly be arranged.

Other matters not included above, if any: 24 h is a rough estimate. Considering that we are quite remote I assume people would rather come for couple of days to use the equipment once a month rather than 4 times for a day.